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Citicoline Sodium and Piracetam is one of the new combinations available in the market for the treatment of patient suffering from Acute Stroke. This combination is also used as a nootropic agents.Only HPLC method is reported for the estimation of these two drugs in combined dosage form found in literature survey.So it was thought of interest to develop and validate the spectroscopic methods for the simultaneous estimation of Citicoline Sodium and Piracetam in combined dosage forms. Also to develop dissolution method to study dissolution profile of these drugs in their combined dosage form.